Journal of Fluorine Chemistry p. 105 - 109 (2014)
Update date:2022-08-28
Topics:
Miloserdov, Fedor M.
Grushin, Vladimir V.
Fluoroform (CHF3) reacts with alkali metal alkoxides MOR (M = Na, K) in the corresponding alcohols ROH (R = Me, Et, i-Pr, t-Bu, and Allyl) at 80-120°C to give orthoformate esters HC(OR)3 in 55-90% yield. Particularly notable is the f
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