Tetrahedron Letters p. 513 - 516 (1993)
Update date:2022-08-28
Topics:
Minami, Tatsuya
Takahashi, Kyoko
Hiyama, Tamejiro
Reduction of β,δ-diketo esters derived from tartaric acid with HAl(i-Bu)2 gave stereoselectively β-hydroxy-δ-keto esters which were reduced with NaBH4 and Et2BOMe to β,δ-syn-dihydroxy esters.This strategy was successfully applied to the synthesis of t-butyl (3R,5S)-6-oxo-3,5-isopropylidenedioxyhexanoate starting from D-tartrate.
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