Canadian Journal of Chemistry p. 1529 - 1535 (1997)
Update date:2022-08-10
Topics:
Beraud
Lessard
Thomalla
The electrocatalytic hydrogenation (ECH) of carvone (1) and limonene (8) at a Raney nickel cathode was studied in aqueous solutions containing a non-micelle-forming surfactant (didodecyldimethylammonium bromide, DDAB). The efficiency of ECH of these substrates was markedly increased compared to that observed previously with micelle-forming surfactants, and this for very low DDAB concentrations, as a consequence of strong adsorption of DDAB on the electrode. For the ECH of 8 in basic medium (pH 10), the major part of organic compounds (60-95%) was shown to be adsorbed on the electrode surface as an organic layer stabilized by an interfacial film of DDAB.
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