`
S. Mazieres, C. Le Roux, M. Peyronneau, H. Gornitzka, N. Roques
SHORT COMMUNICATION
Table 2. Crystal Data for 1·4THF and 2·2THF
1·4THF
2·2THF
Empirical formula
Molecular mass
Crystal system
Space group
C18H32BiClF6O10S2
830.99
monoclinic
P21/c
17.018(2)
18.394(2)
8.960(1)
C9H16Cl2F3O5SSb
485.93
triclinic
¯
P1
˚
a (A)
8.299(2)
9.515(2)
11.395(2)
105.791(2)
96.575(2)
106.136(2)
814.0(3)
2
˚
b (A)
˚
c (A)
α (°)
β (°)
γ (°)
93.232(2)
3
˚
V (A )
2800.3(5)
4
6.626
0.1 ϫ 0.2 ϫ 0.6
0.377188
24516
3985
0.0870
343
0.0646
0.1631
4.498
Z
Abs. coeff. (mmϪ1
Crystal size (mm)
)
2.196
0.3 ϫ 0.5 ϫ 0.6
0.702541
7073
4060
0.0269
190
0.0330
0.0906
2.098
Max. and min. transmission
Reflections collected
Independent reflections
Rint
No. of parameters
R1 [I Ͼ 2σ(I)]
wR2 (all data)
Largest diff. peak (e A
CCDC
Ϫ1
˚
)
199266
199267
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CCDC-199266 (for 1·4THF) and -199267 (for 2·2THF) contain the
supplementary crystallographic data for this paper. These data
can be obtained free of charge at www.ccdc.cam.ac.uk/conts/
retrieving.html [or from the CCDC, 12 Union Road, Cambridge
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Acknowledgments
We gratefully acknowledge the Centre National de la Recherche
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this work.
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