Journal of Organic Chemistry p. 5077 - 5079 (1985)
Update date:2022-08-28
Topics:
Sanchez, Ignacio H.
Mendoza, Serafin
Calderon, Mireya
Larraza, Maria Isabel
Flores, Humberto J.
A total synthesis of (+/-)-perezone (1) proceeding in 18percent overall yield is described.The sequence starts from 5-bromopiperonal (2) and proceeds by way of 7, making use of an AgO-assisted oxidative dealkylation step to unmask the hydroxy-p-quinone-type system characteristic of 1.
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Doi:10.1007/BF00953058
(1985)Doi:10.1016/S0031-9422(00)82656-4
(1981)Doi:10.1021/ja01863a516
(1940)Doi:10.1016/S0040-4039(01)98847-1
(1968)Doi:10.1021/jo00326a016
(1981)Doi:10.1248/cpb.39.2737
(1991)