K.M. Khal’baeva et al. / Journal of Solid State Chemistry 187 (2012) 276–281
281
The lithium cations possess a fairly distorted tetragonal pyrami-
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˚
dal coordination with distances Li–O 2.01(1)–2.25(1) A.
In the structure of LiK2In(MoO4)3, the MoO4 tetrahedra, InO6
octahedra and LiO5 tetragonal pyramids are connected via their
common vertices to form a 3D mixed open framework penetrated
with channels along the a axis (Fig. 5). The channel cavities of the
polyhedral framework contain two kinds of the potassium ions
with coordination numbers 9 and 7 (Table 6).
Acknowledgments
[23] E.I. Get’man, Izomorfnoe Zameshchenie v Molibdatnykh i Volframatnykh
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The authors are grateful to Dr. Dmitry Yu. Naumov and
Dr. Natalia V. Kuratieva for collecting and processing X-ray
single-crystal diffraction data on a Bruker-Nonius X8 Apex CCD
diffractometer. The study has been carried out with a financial
support of the Russian Foundation for Basic Research (Grant No.
03-08-00384) and the International Center for Diffraction Data
(Grant No. 98-15).
[26] SAINT (Version 7.03), SADABS (Version 2.11), Bruker AXS Inc., Madison,
Wisconsin, 2004.
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Appendix A. Supplementary materials
Supplementary materials associated with this article can be
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