Organic Process Research and Development p. 2045 - 2051 (2017)
Update date:2022-08-24
Topics:
Hancker, S?ren
Kreft, Stefanie
Neumann, Helfried
Beller, Matthias
An improved system for the synthesis of N-acyl amino acids via Pd-catalyzed amidocarbonylation is reported. Utilizing inexpensive Pd black gives the industrially important surfactant N-lauroyl sarcosine in excellent yields (95%) on a multi-gram scale. Advantages of the new system include reusability, decreased process temperature, and, importantly, drastically decreased co-catalyst loading.
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