Russian Chemical Bulletin p. 324 - 327 (1997)
Update date:2022-08-29
Topics:
Khisamutdinov
Slovetsky
Golub
Shevelev
Fainzil'berg
Methods for the preparation of α-azidopolynitroalkanes by reactions of polynitroalkanes or α-(difluoroamino)polynitroalkanes with NaN3 were developed. In the case of tetranitromethane, one or two nitro groups can be substituted, depending on the reaction conditions. The reaction of 1,1,1-trinitroethane with NaN3 affords nitro-1,2,3-triazole, together with 1-azido-1,1-dinitroethane. The IR spectra of α-azidopolynitroalkanes were studied.
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