Tetrahedron Letters p. 9141 - 9144 (1994)
Update date:2022-08-17
Topics:
Li, Xun
Provencher, Louis
Singh, Shankar M.
Quantitative free radical addition of perfluoroethyl iodide to propargyl alcohol in the presence of sodium hydrosulfite gave E/Z-2-iodo-4,4,5,5,5-pentafluoro-2-penten-1-ols, which were converted to 4,4,5,5,5-pentafluoropentan-1-ol in one step in excellent yield by catalytic hydrogenation over platinum oxide in the presence of triethylamine. 4,4,5,5,5-Pentafluoropentan-1-thiol was obtained in good yield via modified Mitsunobu reaction of the alcohol.
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Doi:10.1246/cl.1988.1247
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