Journal of Organic Chemistry p. 515 - 518 (1984)
Update date:2022-08-29
Topics:
Cohen, Mark J.
McNelis, Edward
The combination of iodine and iodine pentoxide in methanol was used to convert phenylpropiolic acid and 2-hexynoic acid to the corresponding ketal esters of one less carbon.In both cases, iodoacetylenic compounds were shown to be intermediates.In the case of the phenylpropiolic acid, a diiodoalkene was isolated and shown to be a second intermediate.
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