Phosphorus, Sulfur and Silicon and the Related Elements p. 481 - 484 (2017)
Update date:2022-08-16
Topics:
Ahmadian-Moghaddam, Maryam
Bekhradnia, Ahmadreza
Tatar, Monire
A series of new N-acetyl/thioacetyl-(E)-stilbene benzenesulfonamide derivatives were synthesized regioselectively in moderate to high yields by following a convenient, three-step procedure. The procedure consists of the direct oxidative conversion of a thiol compound to the corresponding sulfonyl chloride using TMSCl/KNO3, followed by a room temperature reaction in a one-pot transformation of the resultant sulfonyl chloride into N-acetyl/thioacetyl sulfonamide, which undergoes a further Pd-catalyzed coupling reaction, giving rise to the stilbene compounds reported for the first time.
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