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ChemComm
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DOI: 10.1039/C7CC05449A
COMMUNICATION
Journal Name
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Notes and references
‡Crystal data for 1: C37H26Cl6FeMo2N10O4S2, Mw = 1199.23,
monoclinic, space group P21/c, a = 11.4437(8) Å, b = 9.1690(7) Å,
c = 40.646(3) Å,
β
= 90.2274(12)°, V = 4264.9(5) Å3, Z = 4, d(calcd)
= 1.868 mg·m−3, T = 150(2) K, 25574 reflections collected, 9705
independent, Rint = 0.0354, R1 = 0.0774, wR2 = 0.1884 for all
data. Crystal data for 2: C36H24Cl4CoMo2N10O4S2, Mw = 1117.38,
monoclinic, space group P21/c, a = 11.4447(5) Å, b = 9.1848(4) Å,
c = 40.5341(18) Å,
β
= 90.2579(9)°, V = 4260.8(3) Å3, Z = 4, d(calcd)
= 1.742 mg·m−3, T = 150(2) K, 27002 reflections collected, 9705
independent, Rint = 0.0478, R1 = 0.0741, wR2 = 0.2356 for all
data. Crystal data for
3: C36H24Cl4NiMo2N10O4S2, Mw = 1117.16,
monoclinic, space group P21/c, a = 11.4015(15) Å, b = 9.1595(12)
Å, c = 40.310(5) Å,
β
= 90.2269(11)°, V = 4209.7(10) Å3, Z = 4,
d(calcd) = 1.763 mg·m−3, T = 150(2) K, 20655 reflections collected,
7705 independent, Rint = 0.0165, R1 = 0.0775, wR2 = 0.2273 for
all data. Crystal data for 3': C43H34Cl2Mo2N14NiS2, Mw = 1132.45,
Triclinic, space group P-1, a = 11.9978(2) Å, b = 12.8594(2) Å, c =
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150(2) K, 29946 reflections collected, 10086 independent, Rint
0.0502, R1 = 0.0489, wR2 = 0.1252 for all data.
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4 | J. Name., 2012, 00, 1-3
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