Tetrahedron Letters p. 2047 - 2050 (1995)
Update date:2022-08-16
Topics:
Mayer, Michael
Ugi, Ivar
Richter, Wolfgang
The phosphorylating reagents CF3P(NMe2)Cl and CF3P(NEt2)Cl are used to phosphorylate the 3'-hydroxyl moiety of several protected 2'-deoxynucleosides yielding the corresponding nucleoside trifluoromethyl phosphonamidites.Their scope and limitations towards amidite activation are investigated but, however, their behavior is completely different to commonly used nucleoside phosphorus amidites.
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