1758
DOTSENKO et al.
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B:COHC.0000023777.35950.cd
15.3486(2) Å, с = 18.6525(3) Å, β = 99.508(2)°, V =
2109.26(5) Å3, Z = 4, dcalc = 1.557 g/cm3, μ(CuKα) =
5.535 mm–1, F(000) = 1008; θ = 3.751°–76.150°, intervals
of reflection indices: 6 ≤ h ≤ –9, 19 ≤ k ≤ –19, 23 ≤ l ≤
–23; the number of measured reflections is 21305, the
number of independent reflections is 4395 (Rint = 0.0521),
the number of reflections with I > 2σ(I) is 4138, the num-
ber of refined parameters is 280, the R-factor [I > 2σ(I)]:
R1 = 0.0310 (wR2 = 0.0835), R-factors for all reflec-
tions: R1 = 0.0327 (wR2 = 0.0850); GOOF by F2 –1.047;
Δρmax/Δρmin = 0.475/–0.411 е Å–3. Some bond lengths and
angles in structure 9 are presented in Table 2. The XRD
data of compound 9 were deposited in the Cambridge
Crystallographic Data Center (CCDC 1861903).
9. Nilov, D.B., Kadushkin, A.V., Solov’eva, N.P.,
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006n05ABEH000640
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Chem. J., 2004, vol. 38, no. 8, p. 451. doi 10.1023/
B:PHAC.0000048910.45523.b7
11. Elgazwy, A.S.S.H. and Soliman, D.H., Open Conf. Proc.
J., 2013, vol. 4, p.77. doi 10.2174/2210289201304010077
12. Gardelly, M., Trimech, B., Belkacem, M.A., Harbach, M.,
Abdelwahed, S., Mosbah, A., Bouajila, J., and Jannet, H.B.,
Bioorg. Med. Chem. Lett., 2016, vol. 26, no. 10, p. 2450.
doi 10.1016/j.bmcl.2016.03.108
FUNDING
This work was supported by the Ministry of Edu-
cation and Science of the Russian Federation (project
no. 4.5547.2017/8.9, V.V. Dotsenko and I.V. Aksenova),
as well as the President of the Russian Federation in the
framework of State Support forYoung Russian Scientists –
Candidates of Sciences (grant no. MK-3089.2018.3).
13. Ali, T.E., Assiri, M.A., Abdel-Kariem, S.M., and
Yahia, I.S., J. Sulfur Chem., 2018. doi 10.1080/
17415993.2018.1455837
14. Mohamed, N.R., Khaireldin, N.Y., Fahmy, A.F., and El-
Sayed, A.A., J. Heterocycl. Chem., 2013, vol. 50, no. 6,
p. 1264. doi 10.1002/jhet.884
CONFLICT OF INTEREST
No conflict of interest was declared by the authors.
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RUSSIAN JOURNAL OF GENERAL CHEMISTRY Vol. 89 No. 9 2019