Tetrahedron Asymmetry p. 771 - 774 (1991)
Update date:2022-08-30
Topics:
Boireau, G.
Deberly, A.
Reduction of the keto group of (-) menthylphenylglyoxalate and (-) menthyl pyruvate can be achieved with high diastereoisomeric excess (80-90percent) using newly synthesized hindered lithium trialkoxyaluminium hydrides in THF at -78 deg C.Hindered borohydrides such as lithium trisiamylborohydride reduce those ketoesters with a lower diastereoselectivity.
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