Catalysis Communications p. 100 - 105 (2017)
Update date:2022-08-16
Topics:
Ye, Yu-Xin
Liu, Wan-Long
Ye, Bao-Hui
A convenient and practical procedure to prepare Pd(II) metallogel as a highly efficient and recyclable catalyst for Suzuki-Miyaura coupling has been developed. Such metallogel shows highly processable and reversible responses to thermal and mechanical stimuli. The xerogel is a highly efficient (0.005?mol% Pd) heterogeneous catalyst for Suzuki-Miyaura couplings with arylhalides and phenylboronic acids in excellent yield in water or ethanol under ambient atmosphere. The reaction could be scaled up to 10?gram scale with 0.001?mol% Pd catalyst loading with 99% yield. The catalyst can be recycled and reused at least seven times without loss of activity.
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