Tetrahedron Letters p. 3011 - 3014 (1996)
Update date:2022-08-11
Topics:
Broddefalk, Johan
Bergquist, Karl-Erik
Kihlberg, Jan
A glycopeptide analogue of the immunodeficient T cell epitope on type II collagen has been prepared by solid phase synthesis. Preparation of a glycosylated amino acid from two monosaccharide units that carried silyl and isopropylidene protective groups and Fmoc 5-hydroxynorvaline was essential for the synthesis. After assembly of the glycopeptide the carbohydrate protective groups were removed simultaneously with acid catalyzed cleavage from the solid phase.
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