Journal of labelled compounds and radiopharmaceuticals p. 959 - 963 (2006)
Update date:2022-08-11
Topics:
Ren
Hesk
McNamara
Koharski
An efficient one step synthesis of [3α-3H]5α- androst-16-en -3β-ol by NaBT4 reduction of a ketone precursor is described. The specific activity of the product was 21.6 Ci/mmol with a radiochemical purity >99%. Synthesis of the precursor, 5α-androst-16- en-3-one, from commercially available 5α-androst-16-en-3α-ol is also presented. Copyright
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