Journal of Organometallic Chemistry p. 21 - 30 (1988)
Update date:2022-08-17
Topics:
Collins, Scott
Kuntz, Bradley A.
Taylor, Nicholas J.
Ward, David G.
The structures of both ethylenebis(η5-tetrahydroindenyl)titanium dichloride (1) and its zirconium analog 2 have been redetermined in the centric space group I2/c (non-standard setting of C2/c) at room temperature.Arguments are presented that suggest that the original space group (Cc) in the published X-ray structures of compounds 1 and 2 was incorrectly selected.An improved modification to the literature route that allows the preparation of multi-gram amounts of 1 and 2 is also described.
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