Tetrahedron Letters p. 3537 - 3539 (2000)
Update date:2022-08-11
Topics:
Soderquist, John A.
Justo De Pomar, Jorge C.
Representative B-substituted-9-BBNs (3) are efficiently prepared from either organolithium or Grignard reagents through their addition to (TIPS)S- 9-BBN (1) which is readily available from TIPSSH and 9-BBN-H. The thermally induced collapse of the intermediate 'ate' complexes (2) produces 3 which is easily isolated in good yield and high purity. (C) 2000 Elsevier Science Ltd.
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