Synthetic Communications p. 2019 - 2027 (1995)
Update date:2022-08-11
Topics:
Wakabayashi
Saito
Sugihara
Sugimura
Murata
β-Elimination of acetic acid was elaborated in our synthetic method of a tricyclo[4.1.0.02,7]hept-4-en-3-one (tropovalene) skeleton. Presented was a new synthetic method of this skeleton, which consists of a reaction sequence of 1,4-addition of propanethiol to bicyclo[3.2.0]hepta-3,6-dien-2-one, photochemical construction of bicyclobutane skeleton, oxidation, and thermal elimination of sulfenic acid.
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