Synthetic Communications p. 3191 - 3194 (1993)
Update date:2022-08-29
Topics:
Cheng
Liu
Intermediates of DBU and TBD, N-(3-aminoproply) - ε -caprolactam and bis- (3-aminopropyl)-amine were prepared by the hydrogenolysis of N-(2-cyanoethyl) - ε - caprolactam and di- (β-cyanoethyl)-amine respectively over Raney-Ni in the presence of NaBH4 under atmospheric pressure with mild condition and good yield.
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Doi:10.1071/CH9950567
(1995)Doi:10.1039/b103508h
(2002)Doi:10.1016/S0022-1139(01)00391-8
(2001)Doi:10.1021/ja01189a030
(1948)Doi:10.1016/0040-4020(61)80005-7
(1961)Doi:10.1007/BF00762080
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