Nucleosides, nucleotides and nucleic acids p. 393 - 400 (2002)
Update date:2022-08-11
Topics:
Rao
Kumar
Chauhan
Garg
Gupta
A rapid and high yielding method for the synthesis of precursors of synthons for DNA synthesis, N-protected 2′-deoxyribonucleosides is described, which occur under mild conditions using microwave irradiation. The desired material, N-protected nucleosides, was obtained in 93-96% yield in few minutes. The final products were then characterized by H-NMR and MALDI-TOF and compared with the standard samples. The method is amenable to small to moderate scale of synthesis.
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