Journal of Organometallic Chemistry p. 26 - 31 (2018)
Update date:2022-08-12
Topics:
Renuka
Gayathri
Novel, simple and efficient catalytic system based on a polymer supported Pd complex of 2,6-bis(benzimidazolyl)pyridine, Pd(PS–BBP)Cl2, was found to be highly active for Suzuki–Miyaura cross-coupling of aryl halides with phenylboronic acids under mild conditions. The catalyst was characterized by CHN analyses, thermogravimetric analyses, BET surface area measurements, ICP-OES, FT-IR and electronic spectral studies. The effect of solvent, base, temperature and catalyst concentration on the coupling reaction of iodobenzene with phenylboronic acid was also investigated. A variety of functional groups are tolerated. The novel catalyst could be recovered in a facile manner from the reaction mixture and could be reused up to seven times without significant loss of catalytic activity.
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