Synthetic Communications p. 3016 - 3025 (2011)
Update date:2022-08-29
Topics:
Cai, Guang-Rong
Guan, Zhi
He, Yan-Hong
A general method for one-pot reaction of hydroquinone derivatives and dienes has been developed. The system of Pb3O4 in tetrahydrofuran- trifluoroacetic acid was found to play dual roles as oxidant for the generation of quinones in situ and as catalyst for the Diels-Alder cycloaddition, which makes the one-pot reaction efficient and easy to carry out. Using this method, a variety of six-membered functionalized carbocyclic compounds can be easily prepared in medium to excellent yields at room temperature. Copyright
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