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19.
Crystal data for 2(dat)·2(4,4`-bpe) (CCDC 1876028): C20H18N2O5
M = 366.36 g/mol, triclinic, Pī, a = 8.2700(8) Å, b = 9.1848(9) Å,
c = 12.4194(12) Å, α = 71.619(5)°, β = 82.065(5)°, γ = 79.191(5)°,
V = 876.19(15) Å3, Z = 2, T = 298(2) K, μ(MoKα) = 0.101 mm-1,
5206 reflections measured, 3148 unique (Rint = 0.0166), R1(obs)
= 0.0604, wR2(all) = 0.1734.
DOI: 10.1039/C9SC05823K
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Crystal data for 2(dat)·(4,4`-tpcb)·THF (CCDC 1895859):
C44H44N4O11 M = 804.83 g/mol: orthorhombic, P212121, a =
10.9162(11) Å, b =
11.3807(11) Å, c =
31.809(3) Å,
V =
3951.8(7) Å3, Z = 4, T = 150(2) K, μ(MoKα) = 0.098 mm-1, 40673
reflections measured, 6949 unique (Rint = 0.0491), R1(obs) =
0.0591, wR2(all) = 0.1643.
Conflicts of interest
There are no conflicts to declare.
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Acknowledgements
The National Science Foundation (L.R.M. DMR-1708673) is
acknowledged for support of the work.
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Notes and references
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