Journal of Fluorine Chemistry p. 61 - 74 (1984)
Update date:2022-08-04
Topics:
Sepiol, Janiusz
Soulen, Robert L.
A three-step high yield synthesis of various 1,3-bis(2-hydroxyhexafluoro-2-propyl)-5-perfluoro-n-alkyl) benzenes is described.Significant improvements in the iodination and perfluoro-alkylation of a perfluoroalkylbenzene diol have been achieved.Copper coupling of straight-chain perfluoroalkyl iodides with the iodobenzene derivative in DMSO gave the desired compounds as DMSO complexes in 78-91 percent yield.
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