Russian Chemical Bulletin p. 699 - 703 (1998)
Update date:2022-08-11
Topics:
Vorogushin
Reshetova
Akhmedov
Ustynyuk
Eremenko
Nefedov
Zinin
The reaction of Cr(CO)6 with 7,7-dichloro-3,4-benzobicyclo[4.1.0]heptane gave the corresponding exo- and endo-chromium tricarbonyl complexes in a ratio of 4.5 : 1 The structures of the resulting compounds were established by NMR spectroscopy, mass spectrometry, and X-ray structural analysis. Reduction of dichlorobenzobicycloheptane and its chromium tricarbonyl complexes with LiAlH4 afforded exo- and endo-7-chloro-3,4-benzobicyclo[4.1.0]heptanes in a 3.5 : 1 ratio.
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