Tetrahedron Letters p. 6353 - 6356 (1985)
Update date:2022-08-17
Topics:
Baird, Mark S.
Gerrard, Michele E.
Searle, Robert J. G.
α-Bromoacrylates, α-bromoacrylonitrile and diethyl alkylidenemalonates all react with bromoform and base under phase transfer conditions to give dibromocyclopropanes.When a γ-bromine is present in a crotonate or an alkylidenemalonate, the intermediate derived by Michael addition of tribromomethylanion is trapped by cyclisation at that position to produce a (tribromomethyl)cyclopropane.
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(1986)