Organic Process Research and Development p. 1423 - 1426 (2017)
Update date:2022-08-16
Topics:
Durrwachter, J. Robert
Neutralization of thionyl chloride in toluene was found to be ineffective with water. A solution is to use an excess of a soluble reagent to consume the thionyl chloride. Butanol was shown to convert thionyl chloride to n-butyl sulfite and hydrogen chloride. An aqueous workup removes any residual hydrogen chloride.
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