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ChemComm
Page 4 of 4
DOI: 10.1039/C5CC06111C
COMMUNICATION
Journal Name
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15 Crystal data for compound 3a: C23H17F7O2, MW = 458.37,
Triclinic, space group Pꢀ1, Final
0.1199, wR2 = 0.2977, indices (all data)
= 0.3230, = 13.635(4) Å, = 13.766(4) Å,
α = 108.215(10)o, β = 105.015(10)o, γ = 110.595(7)o,
2187.5(14) Å3,
= 296(2) K, Z = 4, reflections
collected/unique: 22702/7576 (Rint = 0.0458), number of
observations [>2σ( )]3825, parameters: 577. CCDC: 993055.
R
indices [I > 2σ(I)]
1 = 0.1732, wR
= 14.405(7) Å,
, R1 =
R
R
2
a
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