Synthetic Communications p. 3119 - 3121 (2005)
Update date:2022-08-11
Topics:
Prasad, Maddipati
Nowshuddin, Shaik
Rao
An improved synthesis of N,N′-disuccinimidyl carbonate (DSC) is described where α-pinene is utilized as an efficient scavenger of HCl liberated during the reaction of N-hydroxysuccinimide with triphosgene in THF. The α-pinene hydrochloride formed is soluble in THF and gives very pure DSC in good yields. Copyright Taylor & Francis, Inc.
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