X. Tao et al. / Inorganic Chemistry Communications 14 (2011) 169–171
171
Fig. 3. SEM images showing the morphology and EDX spectrum of the silver deposit obtained from the MOCVD at 350 °C of sample 2b deposited on a Si wafer.
[14] W. Zhang, S.H. Brongersma, O. Richard, B. Brijs, R. Palmans, L. Froyen, K. Maex,
Microelectron. Eng. 76 (2004) 146–152.
[15] L. Gao, P. Harter, C. Linsmeiner, A. Wiltner, R. Emling, D.S. Landsied, Microelectron.
Eng. 82 (2005) 296–300.
(2009ZX02039101-02), Funding of Jiangsu Innovation Program for
Graduate Education (CX10B_100Z), Funding for Outstanding Doctoral
Dissertation in NUAA (BCXJ10-11).
[16] Complex 2a was obtained by N-silver(I) succinimide (0.1379 g, 0.67 mmol) with
trimethylphosphite (0.1661 g, 1.34 mmol) in CH2Cl2 at 0 °C.
A white solid
Appendix A. Supplementary data
product was obtained after removing all volatiles in oil-pump vacuo, Yield: 0.29 g
(95% based on N-silver(I) succinimide). Mp.: 170 °C dec. Anal. calcd. for
C14H26O10Ag2P2N2: C, 25.48; H, 3.97. Found: C, 25.39; H, 3.83. 1 H NMR
(CDCl3, 500 MHZ, ppm): δ 2.61 (s, 4 H, CH2-H), 3.66–3.68 (d, 9 H, CH3O-H,
JPH=12.6 Hz). 13 C{H} NMR (CDCl3, 125 MHZ, ppm): δ 32.1 (CH2), 51.3 (CH3/
CH3O-), δ 191.6 (C=O). IR (KBr) data (cm-1): 3437 (m), 3285 (m), 2939 (m),
2839 (w), 1701 (m), 1618 (s), 1439 (m), 1359 (s), 1269 (s), 1249 (s), 1182 (m),
1012 (s), 790 (m), 761 (m), 669 (m), 571 (w), 526 (m), 451 (m). 31P{H} NMR
(CDCl3, 121 MHZ, ppm): δ 126.8.
Supplementary data to this article can be found online at
doi:10.1016/j.inoche.2010.10.014.
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