Journal of Carbohydrate Chemistry p. 1185 - 1190 (2000)
Update date:2022-08-11
Topics:
Takano, Ryo
Nagai, Tomomi
Wu, Xiaofen
Xu, Xin-Yan
Huy, Nguyen Tien
Kamei, Kaeko
Hara, Saburo
The polysaccharides, curdlan, starch and dextran were sulfated when heated in DMSO with sodium methyl sulfate and a catalytic amount of H2SO4 or with pyridinium methyl sulfate. Use of diminished pressure and anhydrous CaSO4 as a desiccant improved the degree of sulfation and recovery. Under conditions using sodium methyl sulfate, H2SO4 and CaSO4 in vacuo, sulfation at 0-6 was predominant in the cases of curdlan and starch, while sulfation at O-2 and O-3 was preferential in the case of dextran.
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