1042
PISKUNOV et al.
repeated freeze pump thaw cycles. The content of
palladium [11] and bromine [12] in the reaction
product was determined photometrically with an SF-
Maslennikov, V.P., Metalloorg. Khim., 1992, vol. 5,
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7
8
. Bremer, H. and Wendlandt, K.-P., Heterogene Ka-
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4
6 spectrophotometer. Iodine was determined by
argentometric titration [13]. Propylene was deter-
mined chromatographically (Tsvet-106 chromatograph,
thermal conductivity detector, 1000 5-mm glass
column packed with activated carbon, column and
detector temperatures 150 C, carrier gas helium, flow
. Chien, J.C.W. and Dehm, H.S., Chem. Ind., 1961,
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1
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1
1
0. Gordon, A.J. and Ford, R.A., The Chemist’s Com-
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and References, New York: Wiley, 1972.
performed by the resistometric method [14] modified
to exclude contact with air.
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