Phosphorus, Sulfur and Silicon and the Related Elements p. 147 - 153 (1998)
Update date:2022-08-28
Topics:
He, Liang-Nian
Huang, Tian-Bao
Cai, Fei
Chen, Ru-Yu
Lawesson's reagent reacted with phenylthiourea in toluene at 110°C to give a product of ring-opening (2) instead of a 4-membered ring 2a. Its structure was determined by X-ray diffraction analysis. A mechanism is proposed to explain the formation of compound 2. The O-S exchange reaction of Lawesson's reagent with oxamide in acetonitrile was also investigated.
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