Journal of Organic Chemistry p. 6795 - 6799 (2016)
Update date:2022-08-29
Topics:
Tickell, David A.
Lampard, Emma V.
Lowe, John P.
James, Tony D.
Bull, Steven D.
A practically simple derivatization protocol for determining the enantiopurity of chiral diols by 1H NMR spectroscopic analysis is described. Diols were treated with 0.5 equiv of 1,3-phenyldiboronic acid to afford mixtures of diastereomeric boronate esters whose homochiral/heterochiral ratios are an accurate reflection of the diol's enantiopurity.
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