Organic Process Research and Development p. 1753 - 1760 (2018)
Update date:2022-08-18
Topics:
Shalibor, Abdolrahman
Modarresi-Alam, Ali Reza
This study presents a green and efficient process for the preparation of tetraalkylammonium azide applicable in large scale under mild conditions. Moreover, the purity of the product and the reaction yield were significantly high. In this regard, two reactors are compared: batch and flow column reactor. Results demonstrated the greater efficiency of the flow column reactor. Strong base anion exchange resin was used as catalyst. The reusability of the resin was excellent. The environmental factor of this process is 0.85, which is excellent for a chemical process in industrial scale. Accordingly, this method involved almost all principles of Green Chemistry, which is unique for its type.
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