Basic Information | Post buying leads | Suppliers | Cas Database |
Name |
N,N'-Dibenzylethylenediamine |
EINECS | 205-408-4 |
CAS No. | 140-28-3 | Density | 1.028 g/cm3 |
PSA | 24.06000 | LogP | 3.34780 |
Solubility | Slightly soluble in water. | Melting Point |
23-25 °C |
Formula | C16H20N2 | Boiling Point | 373.8 °C at 760 mmHg |
Molecular Weight | 240.348 | Flash Point | 220.5 °C |
Transport Information | UN 2927 | Appearance | N/A |
Safety | 26 | Risk Codes | 22-36/37/38 |
Molecular Structure | Hazard Symbols | Xn | |
Synonyms |
1,2-Ethanediamine,N,N'-bis(phenylmethyl)- (9CI);Ethylenediamine, N,N'-dibenzyl- (7CI,8CI);1,2-Bis(benzylamino)ethane;Benzathine;Benzatin;DBED;N,N'-Bis(phenylmethyl)-1,2-ethanediamine;N,N'-Dibenzyl-1,2-diaminoethane;NSC 5632;NSC 62936; |
Article Data | 72 |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol | 100% |
With sodium tetrahydroborate In ethanol | 95% |
With sodium tetrahydroborate In methanol; dichloromethane | 88% |
N,N'-dibenzoyl-N,N'-dibenzylethylenediamine
N,N'-Dibenzylethylenediamine
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 0.666667h; Heating; | 94% |
1,2-dibenzyl-1,2-diazetin-3-one
N,N'-Dibenzylethylenediamine
Conditions | Yield |
---|---|
With B2H6-THF for 2h; Heating; | 85% |
With diborane In tetrahydrofuran |
Conditions | Yield |
---|---|
Stage #1: benzaldehyde; ethylenediamine With sodium sulfate; triethylamine In ethyl acetate at 20℃; for 14h; Stage #2: With sodium tetrahydroborate In methanol; ethyl acetate for 6h; | 70% |
Stage #1: benzaldehyde; ethylenediamine Stage #2: With sodium tetrahydroborate | 69% |
With sodium tetrahydroborate In methanol at 20℃; Reflux; | 67.6% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether for 1h; Heating; | 51% |
N,N'-bis(benzyliden)ethylendiamine
A
N,N'-Dibenzylethylenediamine
B
N-benzylethylenediamine
Conditions | Yield |
---|---|
With formic acid |
1,2-bis-(benzenesulfonyl-benzyl-amino)-ethane
A
N,N'-Dibenzylethylenediamine
B
N-benzylethylenediamine
Conditions | Yield |
---|---|
With hydrogenchloride at 170 - 180℃; im geschlossenen Rohr; |
formic acid
N-(2-formylaminoethyl)formamide
benzaldehyde
A
N,N'-Dibenzylethylenediamine
B
N-benzylethylenediamine
Conditions | Yield |
---|---|
auch unter Zusatz von Natriumformiat und Kaliumformiat; |
N-(2-formylaminoethyl)formamide
benzaldehyde
A
N,N'-Dibenzylethylenediamine
B
N-benzylethylenediamine
Conditions | Yield |
---|---|
With formic acid |
1. | orl-mus LD50:388 mg/kg | CNCRA6 Cancer Chemotherapy Reports. 52 (1968),579. | ||
2. | ipr-mus LD50:50 mg/kg | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) AD277-689 . | ||
3. | par-mus LD50:80 mg/kg | ANTCAO Antibiotics and Chemotherapy. 4 (1954),633. |