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| Name |
N,N-Dimethyl-1,3-phenylenediamine dihydrochloride |
EINECS | 222-693-0 |
| CAS No. | 3575-32-4 | Density | 1.049g/cm3 |
| PSA | 29.26000 | LogP | 3.52000 |
| Solubility | Soluble in water, hot methanol | Melting Point |
217-220 °C (dec.) |
| Formula | C8H12N2.2(HCl) | Boiling Point | 244.1 °C at 760 mmHg |
| Molecular Weight | 209.119 | Flash Point | 88.8 °C |
| Transport Information | UN 2811 6.1/PG 2 | Appearance | Off-White Crystalline Solid |
| Safety | 36/37/39-45-26 | Risk Codes | 25-36/37/38-43-23/24/25 |
| Molecular Structure |
|
Hazard Symbols |
 T
|
| Synonyms |
1,3-Benzenediamine,N,N-dimethyl-, dihydrochloride (9CI);m-Phenylenediamine, N,N-dimethyl-, dihydrochloride(8CI);3-Dimethylaminoaniline dihydrochloride;N,N-Dimethyl-1,3-benzenediaminedihydrochloride;N,N-Dimethyl-1,3-phenylenediamine dihydrochloride;N,N-Dimethyl-m-phenylenediamine dihydrochloride; |
N,N-Dimethyl-1,3-phenylenediamine dihydrochloride Synthetic route
| Conditions | Yield |
|---|---|
| With sodium carbonate In water at 20℃; for 0.166667h; | 100% |
| With sodium hydrogencarbonate In water; ethyl acetate | |
| With potassium carbonate In water | 3.63 g |
- 3575-32-4
N,N-dimethyl-1,3-phenylenediamine dihydrochloride
| Conditions | Yield |
|---|---|
| With pyridine In chloroform at -20 - 20℃; | 90% |
- 143591-61-1
3-bromo-8-chloro-imidazo[1,2-a]pyrazine
- 936361-36-3
3,8-dibromo-imidazo[1,2-a]pyrazine
- 3575-32-4
N,N-dimethyl-1,3-phenylenediamine dihydrochloride
- 887474-76-2
C14H14BrN5
| Conditions | Yield |
|---|---|
| With N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one at 160℃; for 18h; | 77% |
- 69214-33-1
8-chloroimidazo[1,2-α]pyrazine
- 69214-34-2
8-bromoimidazo[1,2-a]pyrazine
- 3575-32-4
N,N-dimethyl-1,3-phenylenediamine dihydrochloride
- 887474-76-2
C14H14BrN5
| Conditions | Yield |
|---|---|
| With N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one at 160℃; for 18h; | 77% |
- 3575-32-4
N,N-dimethyl-1,3-phenylenediamine dihydrochloride
- 105-53-3
diethyl malonate
- 31136-93-3
2,4-dihydroxy-7-(dimethylamino)quinoline
| Conditions | Yield |
|---|---|
| Stage #1: N,N-dimethyl-1,3-phenylenediamine dihydrochloride With sodium hydroxide In water Stage #2: diethyl malonate at 200℃; Dean-Stark; | 75% |
- 3575-32-4
N,N-dimethyl-1,3-phenylenediamine dihydrochloride
- 105-53-3
diethyl malonate
- 31136-93-3
7-(dimethylamino)-4-hydroxyquinolin-2(1H)-one
| Conditions | Yield |
|---|---|
| Stage #1: N,N-dimethyl-1,3-phenylenediamine dihydrochloride With potassium carbonate In water pH=9 - 10; Stage #2: diethyl malonate In diphenylether Sealed tube; Heating; | 74% |
- 5815-08-7
tert-Butoxybis(dimethylamino)methane
- 3575-32-4
N,N-dimethyl-1,3-phenylenediamine dihydrochloride
| Conditions | Yield |
|---|---|
| Stage #1: tert-Butoxybis(dimethylamino)methane; ethyl 2-(2-ethoxy-2-oxoethyl)-4,5-dimethoxybenzoate at 100℃; for 3h; Stage #2: N,N-dimethyl-1,3-phenylenediamine dihydrochloride With acetic acid at 20℃; for 2h; Stage #3: With sodium hydroxide In ethanol at 80℃; for 1h; | 70% |
- 3575-32-4
N,N-dimethyl-1,3-phenylenediamine dihydrochloride
- 206000-79-5
N-[(3RS)-1-(3-azabicyclo[3.2.2]non-3-yl)carbonylmethyl-5,9-dimethyl-2,3-dihydro-2-oxo-1H-1,4-benzodiazepin-3-yl]-N'-[3-(N,N-dimethyl amino)phenyl]urea hydrochloride
| Conditions | Yield |
|---|---|
| With triethylamine In 1,4-dioxane; water; ethyl acetate; N,N-dimethyl-formamide | 67.1% |
| Conditions | Yield |
|---|---|
| Stage #1: N,N-dimethyl-1,3-phenylenediamine dihydrochloride With potassium carbonate In water for 2h; Stage #2: N,N-Dimethylcarbamoyl chloride With triethylamine In dichloromethane at 0 - 20℃; Schotten-Baumann Reaction; Inert atmosphere; | 67% |
- 3575-32-4
N,N-dimethyl-1,3-phenylenediamine dihydrochloride
- 16588-74-2
3,5-ditrifluoromethylisocyanate
- 1325760-92-6
1-(3,5-bis(trifluoromethyl)phenyl)-3-((3-dimethylamino)phenyl)urea
| Conditions | Yield |
|---|---|
| Stage #1: N,N-dimethyl-1,3-phenylenediamine dihydrochloride With sodium hydroxide In dichloromethane; water Stage #2: 3,5-ditrifluoromethylisocyanate In dichloromethane at 20℃; for 12h; | 66% |
N,N-Dimethyl-1,3-phenylenediamine dihydrochloride Specification
The cas register number of N,N-Dimethyl-1,3-phenylenediamine dihydrochloride is 3575-32-4. It also can be called as N,N-Dimethyl-m-phenylenediamine dihydrochloride and the IUPAC Name about this chemical is 3-N,3-N-dimethylbenzene-1,3-diamine dihydrochloride. It belongs to the following product categories, such as Aromatics Compounds, Aromatics and so on.
Physical properties about N,N-Dimethyl-1,3-phenylenediamine dihydrochloride are: (1)ACD/LogP: 1.05; (2)ACD/LogD (pH 5.5): 0.9; (3)ACD/LogD (pH 7.4): 1.04; (4)ACD/BCF (pH 5.5): 2.64; (5)ACD/BCF (pH 7.4): 3.65; (6)ACD/KOC (pH 5.5): 63.51; (7)ACD/KOC (pH 7.4): 87.81; (8)#H bond acceptors: 2; (9)#H bond donors: 2; (10)#Freely Rotating Bonds: 2; (11)Polar Surface Area: 6.48Å2; (12)Flash Point: 88.8 °C; (13)Enthalpy of Vaporization: 48.11 kJ/mol; (14)Boiling Point: 244.1 °C at 760 mmHg; (15)Vapour Pressure: 0.0309 mmHg at 25°C.
When you are using this chemical, please be cautious about it as the following:
This chemical is toxic by inhalation, in contact with skin and if swallowed and it is irritating to eyes, respiratory system and skin, it also may cause sensitization by skin contact. When you are using it, wear suitable protective clothing, gloves and eye/face protection. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice and in case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
You can still convert the following datas into molecular structure:
(1)Canonical SMILES: CN(C)C1=CC=CC(=C1)N.Cl.Cl
(2)InChI: InChI=1S/C8H12N2.2ClH/c1-10(2)8-5-3-4-7(9)6-8;;/h3-6H,9H2,1-2H3;2*1H
(3)InChIKey: BZJPIQKDEGXVFG-UHFFFAOYSA-N
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