1-amino-2-naphthonitrile

Base Information

• Chemical Name: 1-amino-2-naphthonitrile
• CAS No.: 3100-67-2
• Molecular Formula: C11H8N2
• Molecular Weight: 168.198
• Mol file: 3100-67-2.mol

Synonyms:1-Amino-[2]naphthonitril;1-aminonaphthalene-2-carbonitrile;1-amino-[2]naphthonitrile;1-amino-2-cyanonaphthalene;1-amino-2-naphthylnitrile;1-amino-2-naphthonitrile;

Chemical Property of 1-amino-2-naphthonitrile

Chemical Property:

• Melting Point: 191-192 °C(Solv: water (7732-18-5); benzene (71-43-2))
• Boiling Point: 151-152 °C(Press: 0.3 Torr)
• PKA: -0.32±0.10(Predicted)
• PSA: 49.81000
• Density: 1.22±0.1 g/cm3(Predicted)
• LogP: 2.87488
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

95% ^*data from raw suppliers

1-Amino-2-naphthonitrile ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-amino-2-naphthonitrile

There total 10 articles about 1-amino-2-naphthonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

1-Nitronaphthalene (86-57-7) + methyl 2-cyanoacetate (105-34-0) → 1-amino-2-naphthalenecarbonitrile (3100-67-2)

Guidance literature:

With potassium cyanide; potassium hydroxide; In N,N-dimethyl-formamide; at 60 ℃;

Reference yield: 75.0%

potassium cyanide + 1-Nitronaphthalene (86-57-7) + methyl 2-cyanoacetate (105-34-0) → 1-amino-2-naphthalenecarbonitrile (3100-67-2)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; at 60 ℃;

Reference yield: 60.0%

1-Nitronaphthalene (86-57-7) + ethyl 2-cyanoacetate (105-56-6) → 1-amino-2-naphthalenecarbonitrile (3100-67-2)

Guidance literature:

ethyl 2-cyanoacetate; With potassium cyanide; potassium hydroxide; In N,N-dimethyl-formamide; at 10 ℃; for 0.333333h; Inert atmosphere;

1-Nitronaphthalene; In N,N-dimethyl-formamide; at 60 ℃; for 4h; Inert atmosphere;

upstream raw materials:

benzisatin 3-oxime

2-azidonaphthalene

potassium cyanide

1-Nitronaphthalene

Downstream raw materials:

1-amino-2-(3-methoxybenzoyl)naphthalene

2?chloro?4-phenylbenzoquinazoline

4-phenyl-1H-benzo[h]quinazolin-2-one

2,4‐dichlorobenzo[h]quinazoline

Refernces

• 1、 -. "Aromatic compound and organoelectroluminescent device comprising the compound". Paragraph 0837-0843. . Retrieved 2021/08/31.
• 2、 -. "An electroluminescent compound and an electroluminescent device comprising the same". Paragraph 0541; 0548-0553. . Retrieved 2021/01/30.