5'-Guanylic acid, monosodium salt

Base Information

• Chemical Name: 5'-Guanylic acid, monosodium salt
• CAS No.: 3106-17-0
• Molecular Formula: C₁₀H₁₂N₅O₈P*2Na
• Molecular Weight: 407.187
• Mol file: 3106-17-0.mol

Synonyms:

Chemical Property of 5'-Guanylic acid, monosodium salt

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5'-Guanylic acid, monosodium salt

There total 1 articles about 5'-Guanylic acid, monosodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ disodium guanosine 5'-phosphate (3106-17-0,5550-12-9,13474-02-7,20327-54-2,26714-37-4)

Guidance literature:

In H2O und Me. (Zusatz) bei <40grad;

Reference yield:

guanosine 5'-monophosphate sodium salt (3106-17-0) → β-D-glucose-guanosine-5'-diphosphate diammonium salt

Guidance literature:

Multi-step reaction with 2 steps

1.1: Dowex-50W ion exchange column [H(+) form]

1.2: pH 7

2.1: 1-(benzenesulfonyl)-3-methylimidazolium triflate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.02 h / 20 °C

2.2: 0 - 20 °C

2.3: Dowex-50-W ion-exchange resin [NH₄(+) form]

With 1-(benzenesulfonyl)-3-methylimidazolium triflate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1021/ol203178k

Reference yield:

guanosine 5'-monophosphate sodium salt (3106-17-0) → β-D-galactose-guanosine-5'-diphosphate diammonium salt

Guidance literature:

Multi-step reaction with 2 steps

1.1: Dowex-50W ion exchange column [H(+) form]

1.2: pH 7

2.1: 1-(benzenesulfonyl)-3-methylimidazolium triflate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.02 h / 20 °C

2.2: 0 - 20 °C

2.3: Dowex-50-W ion-exchange resin [NH₄(+) form]

With 1-(benzenesulfonyl)-3-methylimidazolium triflate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1021/ol203178k