Benzonitrile, 2-(phenylethynyl)-

Base Information Edit

Chemical Name:Benzonitrile, 2-(phenylethynyl)-
CAS No.:32183-76-9
Molecular Formula:C15H9N
Molecular Weight:203.243
Hs Code.:
Mol file:32183-76-9.mol

Synonyms:

Suppliers and Price of Benzonitrile, 2-(phenylethynyl)-

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 4 raw suppliers

Chemical Property of Benzonitrile, 2-(phenylethynyl)- Edit

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzonitrile, 2-(phenylethynyl)-

There total 21 articles about Benzonitrile, 2-(phenylethynyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 4387-36-4
2-iodobenzonitrile

: 536-74-3
phenylacetylene

: 32183-76-9
2-(phenylethynyl)benzonitrile

Guidance literature:: With 2C₂H₃O₂^(1-)*Pd⁽²⁺⁾*3Na⁽¹⁺⁾*C₁₈H₁₂O₉PS₃^(3-); potassium tert-butylate; glycerol; at 100 ℃; for 2h; chemoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1002/adsc.201300753

Reference yield: 98.0%

: 873-32-5
2-Chlorobenzonitrile

: 536-74-3
phenylacetylene

: 32183-76-9
2-(phenylethynyl)benzonitrile

Guidance literature:: With potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); (1RS,2RS,3SR,4SR)-1,2,3,4-tetrakis((diphenylphosphanyl)methyl)cyclopentane; In N,N-dimethyl-formamide; at 140 ℃; for 20h;
DOI:10.1016/j.tetlet.2004.09.092

Reference yield: 94.0%

: 2042-37-7
o-cyanobromobenzene

: 536-74-3
phenylacetylene

: 32183-76-9
2-(phenylethynyl)benzonitrile

Guidance literature:: With potassium phosphate; bis(η3-allyl-μ-chloropalladium(II)); N,N,N′,N′-tetra(diphenylphosphinomethyl)-1,2-ethylenediamine; In 1,4-dioxane; at 105 ℃; for 20h; Inert atmosphere;
DOI:10.1007/s10562-012-0796-2