CHLORO-ACETIC ACID TETRAHYDRO-FURAN-2-YL-METHYL ESTER

Base Information

• Chemical Name: CHLORO-ACETIC ACID TETRAHYDRO-FURAN-2-YL-METHYL ESTER
• CAS No.: 702-26-1
• Molecular Formula: C7H11ClO3
• Molecular Weight: 178.6134
• Hs Code.: 2932190090
• Mol file: 702-26-1.mol

Synonyms:Chlor-essigsaeure-tetrahydrofurfurylester;2-(chloroacetoxy-methyl)-tetrahydro-furan;chloro-acetic acid tetrahydrofurfuryl ester;Monochloressigsaeure-tetrahydrofurfurylester;tetrahydrofuran-2-ylmethyl chloroacetate;

Chemical Property of CHLORO-ACETIC ACID TETRAHYDRO-FURAN-2-YL-METHYL ESTER

Chemical Property:

• Vapor Pressure: 0.0242mmHg at 25°C
• Boiling Point: 248.5°C at 760 mmHg
• Flash Point: 106.5°C
• PSA: 35.53000
• Density: 1.201g/cm³
• LogP: 0.94740

Purity/Quality:

98%min ^*data from raw suppliers

Chloro-acetic acid tetrahydro-furan-2-yl-methyl ester ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CHLORO-ACETIC ACID TETRAHYDRO-FURAN-2-YL-METHYL ESTER

There total 3 articles about CHLORO-ACETIC ACID TETRAHYDRO-FURAN-2-YL-METHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

Tetrahydrofurfuryl alcohol (97-99-4) + chloroacetyl chloride (79-04-9) → tetrahydrofurfuryl chloroacetate (702-26-1)

Guidance literature:

With triethylamine; In tert-butyl methyl ether; at 10 - 20 ℃; for 5h;

Reference yield:

Tetrahydrofurfuryl alcohol (97-99-4) + chloroacetic acid (79-11-8) → tetrahydrofurfuryl chloroacetate (702-26-1)

Guidance literature:

Reference yield:

→ tetrahydrofurfuryl chloroacetate (702-26-1)

Guidance literature:

Beim Erhitzen einer Lsg. von Tetrahydrofurfurylalkohol u. Chloressigsaeure in Toluol mit geringen Mengen Toluol-4-sulfonsaeure;

DOI:10.1039/jr9650007162

upstream raw materials:

Tetrahydrofurfuryl alcohol

chloroacetic acid

chloroacetyl chloride

Refernces