Octafluoroadipoyl chloride

Base Information

• Chemical Name: Octafluoroadipoyl chloride
• CAS No.: 336-06-1
• Molecular Formula: C6Cl2F8O2
• Molecular Weight: 326.958
• Hs Code.: 2917190090
• European Community (EC) Number: 689-079-6
• DSSTox Substance ID: DTXSID10379719
• Nikkaji Number: J1.341.542K
• Wikidata: Q81985808
• Mol file: 336-06-1.mol

Synonyms:Octafluoroadipoyl chloride;336-06-1;Perfluoroadipoyl chloride;octafluoroadipoyl dichloride;2,2,3,3,4,4,5,5-octafluorohexanedioyl Dichloride;OCTAFLUOROADIPOYLCHLORIDE;Octafluoroadipic acid dichloride;SCHEMBL1598344;DTXSID10379719;NGSYNEZFBAPQFK-UHFFFAOYSA-N;MFCD00054726;AKOS015852742;Octafluoroadipoyl chloride, AldrichCPR;FT-0676346;A821865

Chemical Property of Octafluoroadipoyl chloride

Chemical Property:

• Boiling Point: 42-45oC 2mm
• PSA: 34.14000
• Density: 1.735±0.06 g/cm3(Predicted)
• LogP: 3.05840
• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 10
• Rotatable Bond Count: 5
• Exact Mass: 325.9147599
• Heavy Atom Count: 18
• Complexity: 344

Purity/Quality:

98%Min ^*data from raw suppliers

OctafluoroadipoylChloride ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C,Xn
• Statements: 34-22
• Safety Statements: 26-36/37/39

MSDS Files:

Useful:

• Canonical SMILES: C(=O)(C(C(C(C(C(=O)Cl)(F)F)(F)F)(F)F)(F)F)Cl

Technology Process of Octafluoroadipoyl chloride

There total 6 articles about Octafluoroadipoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.5%

perfluoroadipic acid (336-08-3) → octafluoroadipoyl chloride (336-06-1)

Guidance literature:

With phosphorus pentachloride;

DOI:10.1016/S0022-1139(00)82657-3

Reference yield:

octafluoro-adipic acid diamide (355-66-8) → octafluoroadipoyl chloride (336-06-1)

Guidance literature:

With 1,4-bis(trichloromethyl)benzene; zinc(II) chloride;

Reference yield:

(2,2,3,3,4,4,5,5-octafluoro)adipic acid dipotassium salt → octafluoroadipoyl chloride (336-06-1)

Guidance literature:

With 1-methyl-pyrrolidin-2-one; benzyltriphenylphosphonium chloride; phosphorus trichloride; In chloroform; at 45 ℃; for 2.5h;

upstream raw materials:

perfluoroadipic acid

octafluoro-adipic acid diamide

perfluoro-1,7-octadiene

1,2,7,8-tetrachloro-1H,2H,7H,8H-tetradecafluoro-octane

Downstream raw materials:

2,2,3,3,4,4,5,5-octafluoro-1,6-hexanediol

Refernces

• 1、 Hudlicky, M.. "SYNTHESIS OF FLUORINATED α-DIKETONES AND SOME INTERMEDIATES". . p. 383 - 406. Retrieved 1981.