Benzamide, N-(1,1,3,3-tetramethylbutyl)-

Base Information

• Chemical Name: Benzamide, N-(1,1,3,3-tetramethylbutyl)-
• CAS No.: 34021-55-1
• Molecular Formula: C15H23NO
• Molecular Weight: 233.354
• Mol file: 34021-55-1.mol

Synonyms:

Chemical Property of Benzamide, N-(1,1,3,3-tetramethylbutyl)-

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzamide, N-(1,1,3,3-tetramethylbutyl)-

There total 10 articles about Benzamide, N-(1,1,3,3-tetramethylbutyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

→ N-(2,4,4-trimethylpentan-2-yl)benzamide (34021-55-1)

Guidance literature:

In 5,5-dimethyl-1,3-cyclohexadiene; for 12h; Reflux;

Reference yield: 65.0%

tert-Octylamine (107-45-9) + Potassium benzoate (582-25-2) → N-(2,4,4-trimethylpentan-2-yl)benzamide (34021-55-1)

Guidance literature:

Potassium benzoate; With 1,3,5-trichloro-2,4,6-triazine; In water; acetonitrile; for 1h;

tert-Octylamine; In water; acetonitrile; at 23 ℃; for 1h;

DOI:10.1021/op980097y

Reference yield: 64.0%

iodobenzene (591-50-4) + 1,1,3,3-tetramethylbutane isonitrile (14542-93-9) → N-(2,4,4-trimethylpentan-2-yl)benzamide (34021-55-1)

Guidance literature:

With water; caesium carbonate; In dimethyl sulfoxide; at 100 ℃; for 24h;

DOI:10.1039/d0nj06301k

upstream raw materials:

2,4,4-trimethylpent-2-ene

benzonitrile

tert-Octylamine

benzoyl chloride

Downstream raw materials:

N-(4-Hydroxy-1,1,3,3-tetramethylbutyl)benzamid

Refernces

• 1、 Loni, Masood,Balmohammadi, Yaser,Dadgar Yeganeh, Reza,Imani, Kaveh,Notash, Behrouz,Bazgir, Ayoob. "A case study of Pd?Pd intramolecular interaction in a benzothiazole based palladacycle; catalytic activity toward amide synthesisviaan isocyanide insertion pathway". supporting information. p. 3290 - 3297. Retrieved 2021/02/26.
• 2、 Choudhary, Shivani,Hamann, Henry J.,Ramachandran, P. Veeraraghavan. "Amine-boranes as Dual-Purpose Reagents for Direct Amidation of Carboxylic Acids". . . Retrieved 2020/11/13.