2-azidobenzoyl Chloride

Base Information Edit

Chemical Name:2-azidobenzoyl Chloride
CAS No.:34897-85-3
Molecular Formula:C7H4ClN3O
Molecular Weight:181.581
Hs Code.:
DSSTox Substance ID:DTXSID701313829
Nikkaji Number:J784.334H
Mol file:34897-85-3.mol

Synonyms:2-azidobenzoyl Chloride;SCHEMBL14435838;NKKFLGZTMQFTCA-UHFFFAOYSA-N;DTXSID701313829;34897-85-3

Suppliers and Price of 2-azidobenzoyl Chloride

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-azidobenzoyl Chloride Edit

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:181.0042895
Heavy Atom Count:12
Complexity:225

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)Cl)N=[N+]=[N-]

Technology Process of 2-azidobenzoyl Chloride

There total 7 articles about 2-azidobenzoyl Chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31162-13-7
2-azidobenzoic acid

: 34897-85-3
o-azidobenzoyl chloride

Guidance literature:: With thionyl chloride; at 80 ℃; for 2h;
DOI:10.1016/S0040-4020(01)89515-6

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 34897-85-3
o-azidobenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: NaNO₂; aq. HCl; NaN₃ / NaOAc

2: SOCl₂

With hydrogenchloride; thionyl chloride; sodium azide; sodium nitrite; sodium acetate;
DOI:10.1016/j.bmcl.2005.06.046

Reference yield:

: 16714-25-3
2-azidobenzaldehyde

: 34897-85-3
o-azidobenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: oxone / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere; Schlenk technique

2: N,N-dimethyl-formamide / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With oxone; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201700928