MoI₂(CO)3(3,5-Me₂py)(PPh₃)

Base Information

• Chemical Name: MoI₂(CO)3(3,5-Me₂py)(PPh₃)
• CAS No.: 117199-12-9
• Molecular Formula: C₂₈H₂₄I₂MoNO₃P
• Molecular Weight: 803.226
• Mol file: 117199-12-9.mol

Synonyms:

Chemical Property of MoI₂(CO)3(3,5-Me₂py)(PPh₃)

Chemical Property:

Purity/Quality:

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Technology Process of MoI₂(CO)3(3,5-Me₂py)(PPh₃)

There total 1 articles about MoI₂(CO)3(3,5-Me₂py)(PPh₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3,5-Lutidine (591-22-0) + MoI2(CO)3(MeCN)2 (102349-56-4) → MoI2(CO)3(3,5-Me2py)(PPh3) (117199-12-9)

Guidance literature:

With triphenylphosphine; In dichloromethane; PPh3 added to a soln. of Mo-complex under a stream of N2 with stirring; after 1 min 3,5-Me2-py was added, mixture stirred for 30 min;; filtered, solvent removed in vacuo, recrystd. from CH2Cl2, elem. anal.;

DOI:10.1016/S0020-1693(00)87509-X

upstream raw materials:

3,5-Lutidine

MoI₂(CO)3(MeCN)2