Butylsec-butylsulfide

Base Information

• Chemical Name: Butylsec-butylsulfide
• CAS No.: 10359-61-2
• Molecular Formula: C8H18 S
• Molecular Weight: 146.297
• Hs Code.: 2930909090
• Mol file: 10359-61-2.mol

Synonyms:Sulfide,butyl sec-butyl (6CI,7CI,8CI); 2-(Butylthio)butane; Butyl sec-butyl sulfide

Chemical Property of Butylsec-butylsulfide

Chemical Property:

• Vapor Pressure: 1.26mmHg at 25°C
• Boiling Point: 179.8°Cat760mmHg
• Flash Point: 55.8°C
• PSA: 25.30000
• Density: 0.836g/cm³
• LogP: 3.31820

Purity/Quality:

98%,99%, ^*data from raw suppliers

BUTYL SEC-BUTYL SULFIDE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of Butylsec-butylsulfide

There total 4 articles about Butylsec-butylsulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C8H17S → butene-2 (107-01-7) + 1-sec-butylsulfanyl-butane (10359-61-2) + n-butyl mercaptyl radical (16812-18-3)

Guidance literature:

With tris-(trimethylsilyl)silane; In toluene; at -70.16 ℃; Further Variations:; Temperatures; Kinetics;

DOI:10.1021/ja027428d

Reference yield:

1-bromo-butane (109-65-9) + s-butyl bromide (78-76-2,5787-31-5) → 1-sec-butylsulfanyl-butane (10359-61-2)

Guidance literature:

Multistep reaction; (i) thiourea, H₂O, (ii) aq. NaOH, (iii) /BRN= 505949/;

DOI:10.1021/ja00868a021

Reference yield:

1-n-butylthio-1-methyl-2-propene (689-90-7) → 1-sec-butylsulfanyl-butane (10359-61-2)

Guidance literature:

With palladium on activated charcoal; ethanol; Hydrogenation;

DOI:10.1039/jr9580002888

upstream raw materials:

1-bromo-butane

1-methyl-1-propanethiol

1-n-butylthio-1-methyl-2-propene

s-butyl bromide

Refernces

• 1、 Chatgilialoglu, Chryssostomos,Altieri, Alessio,Fischer, Hanns. "The kinetics of thiyl radical-induced reactions of monounsaturated fatty acid esters". . p. 12816 - 12823. Retrieved 2002.