Benzeneacetic acid, 1-naphthalenylmethyl ester

Base Information

• Chemical Name: Benzeneacetic acid, 1-naphthalenylmethyl ester
• CAS No.: 36707-29-6
• Molecular Formula: C19H16O2
• Molecular Weight: 276.335
• Mol file: 36707-29-6.mol

Synonyms:

Chemical Property of Benzeneacetic acid, 1-naphthalenylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzeneacetic acid, 1-naphthalenylmethyl ester

There total 2 articles about Benzeneacetic acid, 1-naphthalenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1-naphthalene methanol (4780-79-4) + phenylacetyl chloride (103-80-0) → 1-naphthylmethyl phenylacetate (36707-29-6)

Guidance literature:

With pyridine; In benzene; Ambient temperature;

Reference yield:

→ 1-naphthylmethyl phenylacetate (36707-29-6)

Guidance literature:

Phenylessigsaeurechlorid, α-Naphthylmethanol;

DOI:10.1021/jo00799a600

Reference yield: 84.0%

methanol (67-56-1) + 1-naphthylmethyl phenylacetate (36707-29-6) → phenylacetic acid (103-82-2) + 1-(1-naphthyl)-2-phenylethane (36707-32-1) + 1-(methoxymethyl)naphthalene (5903-23-1)

Guidance literature:

at 20 ℃; Rate constant; Quantum yield; Irradiation;

DOI:10.1021/ja00007a049

upstream raw materials:

1-naphthalene methanol

phenylacetyl chloride

Downstream raw materials:

phenylacetic acid

1-(1-naphthyl)-2-phenylethane

1-(methoxymethyl)naphthalene

Refernces

• 1、 Hilborn, James W.,Pincock, James A.. "Photolysis of the 1-naphthylmethyl ester of substituted phenylacetic acids: intramolecular charge transfer and rates of decarboxylation of arylacyl radicals". . p. 992 - 999. Retrieved 2007/10/02.